建筑用玻化微珠保温混凝土剪力墙抗震结构设计

传统方法主要通过导热系数低的材料和增加墙体厚度来达到抗震效果。该方法不仅浪费能源而且抗震性能较差,因此对建筑用玻化微珠保温混凝土剪力墙抗震结构进行设计,构建玻化微珠保温混凝土本构模型,获得与抗震结构相关的理论数据。根据所获取的数据,选择板壳单元SHELL63作为玻化微珠保温混凝土剪力墙抗震结构单元。依据抗震结构材料参数以及抗震结构单元,采用ANSYS软件模拟构建玻化微珠保温混凝土剪力墙抗震结构。分析实验结果可知,所设计建筑节能抗震结构的抗震性能较好,实际运用价值高。     

Chemical Procedures for Rhenium Extraction from Geological Samples: Optimising the Anion Resin Bead Clean‐up Step

Rhenium–osmium geochronometry for samples with low Re and complex matrices requires improved Re extraction methods. Here, we investigate plausible controls on efficiency and efficacy of Re extraction during our anion resin bead purification. Four different protocols are compared, each isolating a single variable to test. Rhenium concentrations for solutions at each step of each protocol document differences in chemical recovery/yield. The negative‐thermal ionisation mass spectrometry (N‐TIMS) signal intensity serves as a proxy for Re yield and purity. These data document correlations between the N‐TIMS signal intensity and (a) the duration of anion resin bead conditioning prior to loading with Re‐bearing solution, and (b) both duration and strength of nitric acid used during rinsing of the Re‐loaded anion resin bead. The optimal protocol improved Re signal intensity around fourteen times compared with our current Re extraction protocol, an aggregate of 2.4 times improvement in chemical recovery (yield) and 5.8 times improvement in emission efficiency (purity). Repeated N‐TIMS isotopic measurements on our in‐house Re standard solution (1407) verify that our optimal protocol‐3 does not fractionate Re isotopes. The improved anion resin bead method considerably lowers the Re detection limit and allows Re‐Os isotopic analysis of picogram‐level Re hosted in geological samples with complex matrices.     

论珠江三角洲河网的人为影响

文章论述了珠江三角洲河网的发育、演变过程和整治方案。由于人类活动影响,珠江三角洲河网区西、北两江下游放射状河系支汊淤断及消亡,使西、北两江正干均成为单一水道;在两江汇流区内又受绥江三角洲南展而分离开来,只留一条狭窄的小河涌(思贤)连接;由于北江正干的淤积、西江正干刷深,使古代(唐代以前)西江合北江同流向东流入番禺(广州)的形势大变,形成江水反向西流入西江,西江水不能过入广州。由此,西、北两江合成的珠江三角洲主体网河区成为浅水狭窄的小河区,以往主要干流多不复存在,生态环境日益变劣。因此,需要修复河网。关键是把西江大量优质水源(沙少、污染少)引回,过入珠江三角洲网河区,北江水源也需截流使其不再西流入西江;开通北江大堤沿途防西水的闸门(如芦苞、西南、沙口等闸),以便通水通航;在思贤建立新型分水闸,可将西、北两江正干水源恢复到良好生态环境     

Production of carbonate and silica nano-particles in stirred bead milling

This paper presents the experimental results of the mechanical production of silica and carbonate colloidal particles below 100 nm using two types of stirred bead mills (i.e., DCP Superflow 12 and PML H/V). It is shown that the stirred bead mill with very small beads can be used as an efficient equipment for the production of the colloidal particles in nanoscale from the feed materials of several microns in sizes at high energy consumptions. The DCP Superflow mill with high power densities is superior for the effective size reduction and production rate, compared to the conventional PML H/V mill with lower power densities. The smaller particles could be produced by the DCP Superflow mill at the same level of high energy inputs as from the PML H/V mill. The “grinding limit” for the processes in the mills has been discussed.     

长白山火山活动发展阶段及火山灾害评价

长白山地区火山活动划分二个发展阶段：以点一线形式喷发形成的广阔玄武岩台地阶段一焊缝构造发展阶段；中心式大规模喷发形成的锥状火山机构一焊点构造发展阶段，长白山地区乃至吉林东部地区中一新生代以来抬升平均速率81m／Ma及白头山一泉阳一露水河一带中生代以来存在一个火山坳陷盆地。     

GGB-1型X射线荧光光谱分析高频感应熔样机的性能与应用

介绍自行研制的GGB-1型X射线荧光光谱分析高频感应熔样机的特点及性能。采用高频感应加热技术和全自动微机控制技术,设计了温度锁相环控制系统,通过控制高频功率发生器输出振荡电流的大小来控制加热速度和温度,使熔样过程智能化、自动化。研究设计的混匀装置,可同时摇摆与自旋,熔融体形成涡流,使熔融体更均匀。根据X射线荧光光谱分析制样的特点,设计了预氧化过程,更适合于矿石类样品的熔融制样。产品的性能测试结果表明,该熔样机的最高温度为1300℃,温控精度为±2℃,各元素制样精密度优于0.3%(RSD,n=11)。     

CO_2 Density-Raman Shift Relation Derived from Synthetic Inclusions in Fused Silica Capillaries and Its Application

Abstract: The densities of CO2 inclusions in minerals are commonly used to determine the crystallizing conditions of the host minerals. However, conventional microthermometry is difficult to apply for inclusions of small size (< 5–10 μm) or low density. Raman analysis is an alternative method for determining CO2 density, provided that the CO2 density–Raman shift relation is known. This study aims to establish this CO2 density–Raman shift relation by using CO2 inclusions synthesized in fused silica capillaries. By using this newly-developed synthetic technique, we formed pure CO2 inclusions, and their densities were determined by microthermometry. The Raman analysis showed that the relation between CO2 density (D in g/cm3) and the separations (Δ in cm?1) between the two main bands (i.e. Fermi diad bands) in CO2 Raman spectra can be represented by a cubic equation: D (g/cm3)=0.74203(?0.019Δ3+5.90332Δ2?610.79472Δ+21050.30165)?3.54278 (r2=0.99920). Our calculated D value for a given Δ is between those obtained from two previously-reported equations, which were derived from different experimental methods. An example was given in this study to demonstrate that the densities of natural CO2 inclusions that could not be derived from microthermometry could be determined by using our method.     

Peptidomic analysis of Chinese shrimp (Fenneropenaeus chinensis) hemolymph by magnetic bead-based MALDI-TOF MS

Peptides in shrimp hemolymph play an important role in the innate immune response.Analysis of hemolymph will help to detect and identify potential novel biomarkers of microbial infection.We used magnetic bead-based purification(ClinProt system) and matrix-assisted laser desorption/ionization time of flight mass spectrometry(MALDI-TOF MS) to characterize shrimp hemolymph peptides.Shrimp serum and plasma were used as the source of samples for comparative analysis,and it was found that serum was more suitable for shrimp hemolymph peptidomic analysis.To screen potential specific biomarkers in serum of immune-challenged shrimps,we applied magnetic bead-based MALDI-TOF MS to serum samples from 10 immune-challenged and 10 healthy shrimps.The spectra were analyzed using FlexAnalysis 3.0 and ClinProTools 2.1 software.Thirteen peptide peaks significantly different between the two groups were selected as candidate biomarkers of lipopolysaccharide(LPS)-infection.The diagnostic model established by genetic algorithm using five of these peaks was able to discriminate LPS-challenged shrimps from healthy control shrimps with a sensitivity of 90% and a specificity of 100%.Our approach in MALDITOF MS-based peptidomics is a powerful tool for screening bioactive peptides or biomarkers derived from hemolymph,and will help to enable a better understanding of the innate immune response of shrimps.     

重庆忠县翠屏山西晋崖墓出土宝玉石和玻璃饰品的工艺初探

利用显微镜对重庆忠县翠屏山西晋时期崖墓出土的玛瑙珠、琥珀饰品和玻璃珠的表面痕迹进行了显微观察,对它们的加工工艺进行了分析和探讨。其中,玛瑙珠在粗磨过程中应使用了粒径较大、粒度不均匀的石英砂粒,导致玛瑙珠的外形不规整,表面多大而深的凹坑;琥珀饰品的钻孔外缘和表面存在较多应力裂纹,显示当时的玉匠对琥珀的加工尚不能克服琥珀性脆、怕热的缺点;玻璃珠至少可见铸造——切削成形、缠珠和直管切割3种制作工艺。这些饰品的特点反映了西晋时期平民社会所使用的饰品的面貌和工艺水平,为中国古代宝玉石和玻璃器的断代以及工艺研究提供了新的信息。     

X射线荧光光谱法测定高铝粘土中主成分方法研究

使用日本理学ZSX PrimusⅡ型X射线荧光光谱仪,采用熔融玻璃片和经验系数进行基体校正的方法,对我室6件国家标准物质、4件监控样以及用标样和纯值试剂配制的21件混合标准进行组分测定。分析结果表明,此方法能快速、准确测定高铝粘土中主成分Al2O3、SiO2、Fe2O3、TiO2,其准确度和精密度均能达到国家标准方法规定的要求。